Lab: Identify Weak Acid Using Titration Curve

Lab: Identify Weak Acid Using Titration Curve

 

 

 

The lab report must include; Introduction, Hypothesis (if available), Materials and Methods, Results, and Discussion. THIS IS THE LAB needs to be written in essay format 

 

 

  • Acid-base reactions are double-displacement reactions characterized by the formation of an ionic salt and water.
  • A titration is a method of determining the properties of an unknown solution by monitoring the quantity of a solution of known concentration necessary to react with it.
  • The solution with the known concentration in a titration is called the titrant. The solution being studied is called the analyte.
  • A solution with a precisely known concentration is referred to as a standard solution.
  • A titration curve is a plot of pH versus volume of titrant added.
  • The equivalence point in a titration is the point when the amount of titrant added is just enough to react completely with the analyte solution.
  • At the half-equivalence point of a weak acid-strong base titration, the pH of the solution equals the pKa of the weak acid.

Overview

  • In this simulation, you will learn about titration curves and weak acids.
  • You will perform a titration where the analyte is a weak monoprotic acid and the titrant is a strong base.
  • You will create a titration curve.
  • You will use the titration curve to make a tentative identification of the weak acid from its pKa value.
  • You will be analyzing one of the following acids:
Weak Acid pKa
Chloroacetic acid 2.85
Hydrofluoric acid 3.15
Formic acid 3.77
Benzoic acid 4.19
Acetic acid 4.74

Scoring

In this lab simulation, your grade will be based on the following:

  • Answering each question correctly
  • Correctly following the outlined steps of the procedure
  • Making precise and accurate measurements for your Lab Data
  • Calculating precise and accurate values for your Lab Data
  • Reporting your measured and calculated values with the correct number of significant figures

Before you begin

  • The reaction that occurs between an unknown weak monoprotic acid and sodium hydroxide is:

NaOH⁡(a⁢q)+HA⁡(a⁢q)⟶NaA⁡(a⁢q)+H⁢A2⁢O⁡(l)

  • where HA represents the unknown weak monoprotic acid.
  • The titration curve is generated by measuring the pH after incremental additions of base to the acid. A buret is used to precisely measure the amount of base added.
  • Titration of all weak acids with a strong base produces a modified S-curve. The actual shape of the curve depends on the specific acid being titrated and its pKa value.
  • The key features of a titration curve are the half-equivalence point and equivalence point.
Titration curve with pH on the y-axis and volume of NaOH on the x-axis.  The half-equivalence point and equivalence point are labeled.

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